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The ground-glass fitting B shown in Fig. 23(p), p. ) For general work, a very satisfactory apparatus for collecting fractions under reduced pressure is the Perkin triangle C,* which is shown in Fig. 14, together with the requisite fittings for the complete To pump To pump FIG. 14. * G. A. R. Kon (your. Chem. , 1930, 182) described a modification of the Perkin triangle having only two taps instead of the three described above. , Quickfit Works, Stone, Staffs. 32 PRACTICAL ORGANIC CHEMISTRY distillation.

20 PRACTICAL ORGANIC CHEMISTRY with wire gauze. Very rapid drying is thereby obtained, and any acid or basic vapours which may be evolved are absorbed, the interior of the desiccator thus remaining clean and odourless. , an amine hydrochloride, which has been recrystallised from concentrated hydrochloric acid, and which would otherwise fill the desiccator with hydrogen chloride as drying proceeded. , some freshly cut shavings of clean paraffin wax should be added to the calcium chloride in (A) or to the sodium hydroxide in D.

To overcome this difficulty, the liquid is distilled under reduced pressure, so that its boiling-point shall be definitely below its thermal decomposition point. It has already been pointed out that a liquid even when subjected to simple atmospheric distillation may become superheated and then "bump" violently in consequence: this danger is greatly increased during distillation under reduced pressure and therefore a specially designed flask, known as a Claisen flask, is used to decrease the risk of superheating.

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