Chimie Moleculaire Minerale Livres : Chimie moleculaire et by Serge David

By Serge David

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4] W. L. Jorgensen, R. C. Binning, Jr. et B. Bigot, J. Am. Chem. , 103 (1981) 43934399. [5] W. L. Jorgensen et M. Ibrahim, J. Am. Chem. , 103 (1981) 3976-3985. [6] E. L. Eliel, K. D. Hargrave, K. M. Pietrusiewicz et M. Manoharan, J. Am. Chem. , 104 (1982) 3635-3643. [7] M. C. Planje, L. H. Toneman et G. Dallinga, Rec. Trav. , 84 (1965) 232-240. [8] C. B. T. Sepp, J. Org. , 32 (1967) 607-611. [9] C. T. Bishop et E P. Cooper, Can. J. , 41 (1963) 2743-2758. [IO] P. L. Durette et D. Horton, Adv. Curb.

Ce léger excès est donc compensé lors de l’élaboration du cristal, qui sélectionne la conformation tétraéquatoriale en solution et déplace l’équilibre totalement vers la gauche. 5 favorise-t-elle un empilement compact. Ceci dit, lorsque la conformation en solution d’une molécule apparaît unique en solution, avec nos méthodes actuelles d’observation, dans la vaste majorité des cas, c’est celle-ci que l’on retrouve dans le cristal. 3 CONFORMATION EN SOLUTION : RÉSONANCE MAGNETIQUE NUCLEAIRE DU PROTON On a déjà mentionné au chapitre premier l’utilisation de la résonance magnétique nucléaire à l’étude des équilibres anomériques, par analyse de la partie du spectre relative aux protons anomériques.

J. Angyal, Adv. , 42 (1984) 15-68 ; 49 (1991) 19-35. [4] K. B. Hicks, Adv. Curbohydr: Chern. , 46 (1988) 17-72. [5] S. Honda, S. Suzuki et K. Kakehi, J. Chrornutogr, 291 (1984) 317-325. 161 R. Barker et A. S. Serianni, Acc. Chern. , 19 (1986) 307-313. [7] M. J. King-Morris et A. S. Serianni, J. Am. Chern. , 109 (1987) 3501-3508. [8] H. S. Isbell et W. Pigman,Adv. Curbohydr. , 23 (1968) 11-57 ; 24 (1969) 13-65. [9] E Hucho et K. Wallenfels, Eux J. , 23 (1971) 489-496. 1 SYMBOLES DE CONFORMATION : PYRANOSES Les conformations remarquables du cycle oxane (tétrahydropyranne) des pyranoses sont les mêmes que celles du cyclohexane.

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